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Correction
N
one
Autostore tab
File Storage: Storage OFF
4. Click the 'Goto' button to open the 'Goto wavelength' dialog box. Enter '500' in
the wavelength field and click OK. The instrument will then drive to 500 nm.
Zero %R error check
1. With the transmission ports uncovered, place the large reference plate over the
reflectance port.
2. From the main 'Scan' dialog box, click the Zero button and wait for the
instrument to zero.
3. Remove the reference plate so the beam is going straight through the sphere
into the Extended Sample Compartment. Close the sample compartment, the
reading should not be greater than 0.5%R. If it is then check the alignment of
the beam through the sphere (adjust M2 as necessary), check that the lens is
clean and free from dust, and ensure that the beam is not clipping the
reflectance port.
Electronic calibration check
1. Place the large reference plate over the reflectance port, close the sample
compartment and then zero the instrument
2. Block the beam with a blanking plate (a large solid object) placed in front of
the transmission port of the sphere.
3. The reading should be less than 0.5%R. If it is not, use the Calibration menu
item in the Validate application. Refer to the Calibration
section for further
details.
Specular component exclusion check
1. Position the sphere cap so the 'D' is facing up.
2. Place the large reference plate over the reflectance port.
3. Click the Goto button to open the Goto wavelength dialog box. Enter '500' in
the Wavelength field and click OK. The instrument will then drive to 500 nm.
Close the sample compartment lid.
4. Click the Zero button and wait for the instrument to zero.
5. Place the supplied mirror over the reflectance port, and close the sample
compartment. Note the reading. If the reading is greater than 1.5%R, then
either the specularly reflected beam is not exiting the sphere at the
transmission port, dirt on the lens is scattering the beam and creating a 'halo'
effect on the reflectance port, or the sample mirror does not have a good
specular surface. If the reading is greater than 1.5%R, you should repeat the
check for the specular component as detailed in the Checking for the specular
component section.
6. Rotate the sphere cap 180° so that the 'S' mark is facing up. When the sample
compartment is closed, the reading should be approximately 90%.
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